Structures published

Total: 659

2-Nitrodiphenylamine

C₁₂H₁₀N₂O₂

McWilliam, Susan A.Skakle, Janet M. S.Wardell, James L.Low, John Nicolson Glidewell, Christopher

Acta Crystallographica Section C (2001) 57, 8 946-948

a=14.7077(5)Å b=10.1602(4)Å c=6.7878(2)Å

α=90.00° β=90.00° γ=90.00°

2-Iodo-4-nitroaniline

C₆H₅IN₂O₂

McWilliam, Susan A.Skakle, Janet M.S.Low, John N.Wardell, James L.Garden, Simon J.Pinto, Angelo C.Torres, Jose C.Glidewell, Christopher

Acta Crystallographica Section C (2001) 57, 8 942-945

a=7.4215(5)Å b=12.6755(9)Å c=16.4638(11)Å

α=90.00° β=90.00° γ=90.00°

N,N'-Bis[tris(hydroxymethyl)methyl]ethanediamide

C₁₀H₂₀N₂O₈

Ross, Jennifer N.Low, John N.Fernandes, Christiane Wardell, James L.Glidewell, Christopher

Acta Crystallographica Section C (2001) 57, 8 949-951

a=21.4097(3)Å b=6.1559(6)Å c=10.0605(13)Å

α=90° β=90° γ=90°

4-Methyl-3-nitroaniline

C₇H₈N₂O₂

Zakaria, Choudhury M.Low, John N.Skakle, Janet M. S.McWilliam, Susan A.Wardell, James L.Glidewell, Christopher

Acta Crystallographica Section C (2001) 57, 10 1207-1208

a=8.2473(7)Å b=7.5676(7)Å c=23.7798(16)Å

α=90° β=91.717(5)° γ=90°

2-Amino-6-nitrobenzothiazole

C₇H₅N₃O₂S

Glidewell, Christopher Low, John N.McWilliam, Susan A.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2001) 57, 10 1209-1211

a=3.7715(2)Å b=15.6399(8)Å c=13.3484(9)Å

α=90° β=93.252(2)° γ=90°

Dichlorobis(4-methylpentane-2-onato-C^4^,O)tin(IV)

C₁₂H₂₂Cl₂O₂Sn

Howie, R. Alan Wardell, James L.

Acta Crystallographica Section C (2001) 57, 9 1041-1043

a=9.6242(2)Å b=11.9846(3)Å c=14.5866(3)Å

α=90° β=106.1048(17)° γ=90°

Bis(4-methylpentan-2-onato-C^4^,O)(2-thioxo-1,3-dithiole-4,5-dithiolato- S,S')tin(IV)

C₁₅H₂₂O₂S₅Sn

Howie, R. Alan Wardell, James L.

Acta Crystallographica Section C (2001) 57, 9 1041-1043

a=11.0670(2)Å b=15.4499(4)Å c=12.2682(2)Å

α=90° β=94.7892(16)° γ=90°

4-Iodo-2-methyl-5-nitroaniline

C₇H₇IN₂O₂

Garden, Simon J.Glidewell, Christopher Low, John N.McWilliam, Susan A.Pinto, Angelo C.Skakle, Janet M. S.Torres, Jose C.Wardell, James L.

Acta Crystallographica Section C (2001) 57, 10 1212-1214

a=13.5264(7)Å b=4.2773(2)Å c=16.3725(8)Å

α=90° β=109.8350(10)° γ=90°

6,6-Diphenyl-6,7-dihydro-5H-1,3,4,8-tetrathia-6-stannaazulene-2-thione

C₁₇H₁₄S₅Sn

Harrison, William T. A.Howie, R. Alan Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2002) 58, 6 m351-m354

a=8.6706(5)Å b=8.5319(6)Å c=13.3143(9)Å

α=90° β=103.8400(10)° γ=90°

6,6'-spirobi[6,7-dihydro-5H-1,3,4,8-tetrathia-6-stannaazulene]-2,2'-dithione

C₁₀H₈S₁₀Sn

Harrison, William T. A.Howie, R. Alan Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2002) 58, 6 m351-m354

a=11.3973(4)Å b=14.2749(5)Å c=12.5609(5)Å

α=90° β=114.6250(10)° γ=90°

N-(2-Iodo-4-nitrophenyl)-4-iodobenzamide

C₁₃H₈I₂N₂O₃

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2003) 59, 11 o636-o637

a=15.6188(5)Å b=4.72530(10)Å c=19.7669(7)Å

α=90° β=104.0822(12)° γ=90°

Bis(acetonitrile-κN)[(1RS,4RS,8SR,11SR)-1,4,8,11-tetraazatetradecane- κ^4^N]copper(II) bis{tetrakis[3,5-bis(trifluoromethyl)phenyl]borate} 0.31-hydrate

C₁₄H₃₀CuN_62,2C₃₂H₁₂BF_241,0.31H₂O

Janet M. S. Skakle Marcus V. D. Rangel e Silva James L. Wardell Solange M. S. V. Wardell

Acta Crystallographica Section C (2003) 59, 10 m413-m415

a=25.7320(6)Å b=18.3516(4)Å c=17.5412(4)Å

α=90.00° β=90.00° γ=90.00°

2-(3-nitrophenylaminocarbonyl)benzoic acid

C₁₄H₁₀N₂O₅

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2006) 62, 1 o5-o7

a=4.0511(9)Å b=12.076(3)Å c=12.771(3)Å

α=90.00° β=90.287(12)° γ=90.00°

Ethyl 5-cyano-2,6-dimethyl-4-(5-nitro-2-furyl)-1,4-dihydropyridine-3-carboxylate

C₁₅H₁₅N₃O₅

Quesada, Antonio DaSilva, Jacqueline A.Squella, Juan A.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 1 o8-o12

a=8.0214(3)Å b=13.7477(4)Å c=13.2847(4)Å

α=90.00° β=95.3019(17)° γ=90.00°

Diethyl 2,6-dimethyl-4-(5-nitro-2-furyl)-1,4-dihydropyridine-3,5-dicarboxylate

C₁₇H₂₀N₂O₇

Quesada, Antonio DaSilva, Jacqueline A.Squella, Juan A.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 1 o8-o12

a=8.0511(2)Å b=15.173(4)Å c=14.470(4)Å

α=90.00° β=105.760(2)° γ=90.00°

2,6-dimethyl-4-(5-nitro-2-furyl)-1,4-dihydropyridine-3,5-dicarbonitrile

C₁₃H₁₀N₄O₃

Quesada, Antonio DaSilva, Jacqueline A.Squella, Juan A.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 1 o8-o12

a=9.5651(3)Å b=7.5735(2)Å c=17.6385(5)Å

α=90.00° β=96.2570(13)° γ=90.00°

Methyl 3,5-dinitrobenzoate

C₈H₆N₂O₆

Vasconcelos, Thatyana R. A.de Souza, Marcus V. N.Wardell, Solange M. S. V.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 1 o26-o29

a=4.5664(4)Å b=18.727(2)Å c=10.8416(10)Å

α=90.00° β=101.787(6)° γ=90.00°

Benzyl 3,5-dinitrobenzoate?

C₁₄H₁₀N₂O₆

Vasconcelos, Thatyana R. A.de Souza, Marcus V. N.Wardell, Solange M. S. V.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 1 o26-o29

a=20.8531(5)Å b=20.8531(5)Å c=6.0377(2)Å

α=90.00° β=90.00° γ=90.00°

3-(3-Nitrophenylaminocarbonyl)propionic acid

C₁₀H₁₀N₂O₅

Wardell, James L.Skakle, Janet M. S.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 1 o45-o46

a=6.6765(4)Å b=19.7961(13)Å c=9.0675(5)Å

α=90.00° β=113.595(4)° γ=90.00°

Pyrrole-2-carbaldehyde isonicotinoylhydrazone monohydrate

C₁₁H₁₀N₄O_,H₂O

Wardell, Solange M. S. V.de Souza, Marcus V. N.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 1 o47-o49

a=6.4224(3)Å b=7.2115(5)Å c=23.6073(16)Å

α=90.00° β=90.00° γ=90.00°

2,4-difluorobenzaldehyde benzoylhydrazone

C₁₄H₁₀F₂N₂O

Wardell, Solange M. S. V.de Lima Ferreira, Marcelle de Souza, Marcus V. N.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 3 o118-o121

a=10.1310(3)Å b=17.2172(6)Å c=14.4288(5)Å

α=90.00° β=103.957(2)° γ=90.00°

(E,E)-N,N'-bis(4-nitrobenzylidene)butane-1,4-diamine

C₁₈H₁₈N₄O₄

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2006) 62, 1 o1-o4

a=7.1162(4)Å b=7.1895(2)Å c=9.1695(4)Å

α=83.210(3)° β=78.920(2)° γ=64.808(3)°

(E,E)-N,N'-bis(4-nitrobenzylidene)hexane-1,6-diamine

C₂₀H₂₂N₄O₄

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2006) 62, 1 o1-o4

a=6.1908(3)Å b=4.9761(2)Å c=30.1095(15)Å

α=90.00° β=94.331(3)° γ=90.00°

2,4-dichlorobenzaldehyde benzoylhydrazone

C₁₄H₁₀Cl₂N₂O

Wardell, Solange M. S. V.de Lima Ferreira, Marcelle de Souza, Marcus V. N.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 3 o118-o121

a=10.5093(5)Å b=17.6499(9)Å c=14.7982(5)Å

α=90.00° β=104.732(2)° γ=90.00°

Bis(tetrabutylammonium) tris(2-oxo-1,3-dithiole-4,5-dithiolato)stannate(IV)

2C₁₆H₃₆N_,C₉O₃S₁₂Sn₂

Comerlato, Nadia M.Ferreira, Glaucio B.Harrison, William T. A.Howie, R. Alan Wardell, James L.

Acta Crystallographica Section C (2005) 61, 3 m139-m143

a=10.7732(4)Å b=18.3479(7)Å c=27.5862(9)Å

α=90° β=90° γ=90°

Bis(tetraphenylphosphonium) tris(2-oxo-1,3-dithiole-4,5-dithiolato)stannate(IV)

2C₂₄H₂₀P_,C₉O₃S₁₂Sn₂

Comerlato, Nadia M.Ferreira, Glaucio B.Harrison, William T. A.Howie, R. Alan Wardell, James L.

Acta Crystallographica Section C (2005) 61, 3 m139-m143

a=14.2844(2)Å b=26.4828(4)Å c=15.4538(2)Å

α=90° β=90.4168(6)° γ=90°

5-benzylidene-1,3-dimethylpyrimidine-2,4,6(1H,3H,5H)-trione

C₁₃H₁₂N₂O₃

Rezende, Marcos C.Dominguez, Moisés Wardell, James L.Skakle, Janet M. S.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 5 o306-o311

a=6.1293(3)Å b=13.9633(8)Å c=13.2727(8)Å

α=90.00° β=97.688(4)° γ=90.00°

5-(4-methoxybenzylidene)-1,3-dimethylpyrimidine-2,4,6(1H,3H,5H)-trione

C₁₄H₁₄N₂O₄

Rezende, Marcos C.Dominguez, Moisés Wardell, James L.Skakle, Janet M. S.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 5 o306-o311

a=7.5906(6)Å b=8.2989(7)Å c=10.3010(10)Å

α=92.544(6)° β=93.074(5)° γ=104.456(6)°

5-[4-(dimethylamino)benzylidene]-1,3-dimethylpyrimidine-2,4,6(1H,3H,5H)-trione

C₁₅H₁₇N₃O₃

Rezende, Marcos C.Dominguez, Moisés Wardell, James L.Skakle, Janet M. S.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 5 o306-o311

a=8.6187(2)Å b=8.8451(3)Å c=9.0566(3)Å

α=82.2980(18)° β=84.465(2)° γ=82.365(2)°

5-[3,5-di-tert-butyl-4-hydroxybenzylidene]-1,3-dimethylpyrimidine- 2,4,6(1H,3H,5H)-trione

C₂₁H₂₈N₂O₄

Rezende, Marcos C.Dominguez, Moisés Wardell, James L.Skakle, Janet M. S.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 5 o306-o311

a=9.6040(3)Å b=11.6691(4)Å c=17.2905(6)Å

α=97.4860(16)° β=92.5540(18)° γ=90.006(2)°

1-(2-Iodophenyl)-4-(3-nitrophenyl)-2,3-diaza-1,3-butadiene

C₁₄H₁₀IN₃O₂

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2005) 61, 5 o312-o316

a=7.2969(3)Å b=7.3235(3)Å c=13.7939(6)Å

α=97.405(2)° β=100.410(2)° γ=107.590(3)°

1-(2-Iodophenyl)-4-(4-nitrophenyl)-2,3-diaza-1,3-butadiene

C₁₄H₁₀IN₃O₂

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2005) 61, 5 o312-o316

a=27.9470(11)Å b=8.0563(3)Å c=13.7464(5)Å

α=90.00° β=117.4250(10)° γ=90.00°

1-(2-Iodophenyl)-4-(2-nitrophenyl)-2,3-diaza-1,3-butadiene

C₁₄H₁₀I_1.118N_2.882O_1.764

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2005) 61, 5 o312-o316

a=15.3033(8)Å b=3.7952(3)Å c=23.3097(16)Å

α=90.00° β=97.836(4)° γ=90.00°

2-bromo-6-chloro-4-nitroaniline

C₆H₄Br_0.90Cl_1.10N₂O₂

Glidewell, Christopher Low, John N.Skakle, Janet M. S.Wardell, James L.

Acta Crystallographica Section C (2005) 61, 5 o336-o338

a=3.8052(3)Å b=17.9667(13)Å c=12.0417(9)Å

α=90.00° β=93.224(2)° γ=90.00°

4-Cyanobenzaldehyde isonicotinoylhydrazone monohydrate

C₁₄H₁₀N₄O_,H₂O

Souza, Marcus V. N. de Wardell, Solange M. S. V.Wardell, James L.Low, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 3 o166-o168

a=6.9692(2)Å b=12.3802(5)Å c=14.5513(7)Å

α=90.00° β=90.00° γ=90.00°

Bis{di-μ-hydroxidobis[fac-aquatribromidotin(IV)]} heptahydrate

Br₆H₆O₄Sn_2,3.5(H₂O)

de Lima, Geraldo M.Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 3 i18-i19

a=9.9652(2)Å b=14.0027(3)Å c=14.5230(3)Å

α=64.8591(13)° β=69.9803(13)° γ=75.0492(15)°

N-(4-Chlorophenyl)-1,1,1-trifluoro-N- (trifluoromethylsulfonyl)methanesulfonamide

C₈H₄ClF₆NO₄S₂

Boechat, Núbia dos Santos Lages, Adriana Kover, Warner B.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 3 o506-o507

a=11.5998(3)Å b=13.4423(4)Å c=9.0548(2)Å

α=90° β=108.014(2)° γ=90°

7-Chloro-4-[(E)-2-(2-methoxybenzylidene)hydrazin-1-yl]quinoline monohydrate

C₁₇H₁₄ClN₃O_,H₂O

de Souza, Marcus V. N.Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.Kaiser, Carlos R.

Acta Crystallographica Section E (2010) 66, 3 o698-o699

a=3.9202(2)Å b=24.5084(17)Å c=16.1212(11)Å

α=90° β=91.639(4)° γ=90°

(E)-1-Phenyl-2-({5-[(1E)-(2-phenylhydrazin-1-ylidene)methyl]- 2-thienyl}methylidene)hydrazine

C₁₈H₁₆N₄S

de Lima, Geraldo M.Harrison, William T. A.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 3 o504-o505

a=15.6495(6)Å b=15.6495(6)Å c=5.9335(10)Å

α=90° β=90° γ=120°

meso-1-{[2-(Propane-1-sulfinyl)ethane]sulfinyl}propane

C₈H₁₈O₂S₂

Wardell, Solange M. S. V.Wardell, James L.de Lima, Geraldo M.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 3 o647-o648

a=11.9794(9)Å b=5.2190(3)Å c=8.7618(5)Å

α=90° β=97.191(5)° γ=90°

4-(3,3-Dimethylperhydro-1,3-oxazolo[3,4-a]pyridin-1-yl)-2,8- bis(trifluoromethyl)quinoline

C₂₀H₂₀F₆N₂O

Wardell, James L.Wardell, Solange M. S. V.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 3 o700-o701

a=8.4192(3)Å b=9.1833(4)Å c=12.4424(4)Å

α=87.912(2)° β=86.666(2)° γ=78.804(2)°

2-Chloro-6,6-dimethyl-5,6-dihydroindazolo[2,3-c]quinazoline

C₁₆H₁₄ClN₃

Boechat, Núbia dos Santos Lages, Adriana Kover, Warner B.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 3 o521-o522

a=9.8636(2)Å b=10.7971(2)Å c=13.2387(3)Å

α=93.4830(10)° β=100.3910(10)° γ=104.4190(10)°

Bis(2-{[2,8-bis(trifluoromethyl)quinolin-4-yl](hydroxy)methyl}piperidin-1-ium) tetrachloridodiphenylstannate(IV)

2(C₁₇H₁₇F₆N₂O)_,C₁₂H₁₀Cl₄Sn₂

Wardell, James L.Wardell, Solange M. S. V.Tiekink, Edward R. T.de Lima, Geraldo M.

Acta Crystallographica Section E (2010) 66, 3 m336-m337

a=8.5578(4)Å b=9.1479(7)Å c=15.9866(11)Å

α=104.739(3)° β=91.671(4)° γ=97.622(4)°

Μ-Acetato-bis(μ-2-{[(3-chloro-2-hydroxypropyl)(2- pyridylmethyl)amino]methyl}phenolato)dinickel(II) chloride

C₃₄H₃₉Cl₂N₄Ni₂O_6,Cl

Tiekink, Edward R. T.Wardell, James L.Fernandes, Christiane Horn, Jr, Adolfo Skakle, Janet M. S.

Acta Crystallographica Section E (2010) 66, 5 m566-m567

a=19.0992(6)Å b=18.0097(5)Å c=10.1288(3)Å

α=90° β=90° γ=90°

4-[(Dimethylamino)methylidene]-2-(4-nitrophenyl)-1,3-oxazol-5(4H)-one

C₁₂H₁₁N₃O₄

Romeiro, Gilberto A.Ribeiro, Carlos M. R.Wardell, Solange M. S. V.Wardell, James L.Ng, Seik Weng Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 6 o1450-o1451

a=9.5313(2)Å b=9.5204(3)Å c=13.0349(4)Å

α=90° β=106.661(2)° γ=90°

1,3-Bis(4-bromophenyl)imidazolium chloride dihydrate

C₁₅H₁₁Br₂N_2,Cl_,2(H₂O)

Garden, Simon J.Gama, Paola E.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.Howie, R. Alan

Acta Crystallographica Section E (2010) 66, 6 o1438-o1439

a=17.8377(7)Å b=17.8377(7)Å c=5.12700(10)Å

α=90° β=90° γ=90°

3-[(E)-(7-Chloro-4-quinolyl)hydrazonomethyl]benzonitrile mono hydrate

C₁₇H₁₁ClN_4,H₂O

de Ferreira, Marcelle L.de Souza, Marcus V. N.Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3239-o3240

a=8.7406(2)Å b=9.8587(3)Å c=10.2301(2)Å

α=110.8897(15)° β=93.4341(16)° γ=110.6766(15)°

C₁₆H₁₄N₂O₂

Carvalho, Samir A.da Silva, Edson F.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3118

a=15.9696(7)Å b=10.4563(5)Å c=8.3162(2)Å

α=90° β=102.072(3)° γ=90°

4-[(2-Chloroethyl)amino]quinolinium chloride monohydrate

C₁₁H₁₂ClN_2,Cl_,H₂O

de Souza, Marcus V. N.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3120-o3121

a=18.7513(7)Å b=14.1030(5)Å c=4.6060(10)Å

α=90° β=90° γ=90°

4-(Pyrimidin-2-yl)-1-thia-4-azaspiro[4.5]decan-3-one

C₁₂H₁₅N₃OS

Neuenfeldt, Patrícia D.Drawanz, Bruna B.Cunico, Wilson Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3190-o3191

a=6.2466(2)Å b=8.6748(2)Å c=22.0439(6)Å

α=90° β=95.6980(10)° γ=90°

7-Chloro-4-[(E)-(3-chlorobenzylidene)hydrazinyl]-1λ^4^-quinolinium 3-chlorobenzoate

C₁₆H₁₂Cl₂N_3,C₇H₄ClO₂

de Souza, Marcus V. N.Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3204-o3205

a=8.8777(2)Å b=10.7064(3)Å c=11.9807(3)Å

α=112.5318(12)° β=91.6382(15)° γ=97.4362(15)°

2-[(E)-(1H-Pyrrol-2-ylmethylidene)hydrazinyl]pyridine monohydrate

C₁₀H₁₀N_4,H₂O

de Lima, Geraldo M.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3241

a=5.6479(3)Å b=7.4383(4)Å c=24.4233(11)Å

α=90° β=103.300(3)° γ=90°

Bis[2-(ethoxycarbonylamino)ethanaminium] hexabromidostannate

2(C₅H₁₃N₂O₂)_,Br₆Sn₂

Howie, R. Alan de Lima, Geraldo M.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 m1562

a=21.8907(5)Å b=7.4428(2)Å c=15.5318(4)Å

α=90° β=105.934(2)° γ=90°

(Dimethyl sulfoxide-κO)diphenyl(3-thioxo-3H-1,2-dithiole-4,5-dithiolato- κ^2^S^4^,S^5^)tin(IV)

C₁₇H₁₆OS₆Sn

Comerlato, Nadia M.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 m1592-m1593

a=11.1420(5)Å b=15.7237(6)Å c=11.9646(6)Å

α=90° β=96.892(2)° γ=90°

Bis[1-(isopropylideneamino)guanidinium] bis(3-nitrobenzoate) monohydrate

2(C₄H₁₁N₄)_,2(C₇H₄NO₄)_,H₂O

Skakle, Janet M. S.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3221-o3222

a=16.5833(6)Å b=22.2457(10)Å c=7.5424(3)Å

α=90° β=92.232(2)° γ=90°

(S)-6-Chloro-4-cyclopropylethynyl-4-trifluoromethyl- 1H-3,1-benzoxazin-2(4H)-one

C₁₄H₉ClF₃NO₂

Cuffini, Silvia Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3170-o3171

a=8.1403(4)Å b=13.5859(11)Å c=24.962(2)Å

α=90° β=90° γ=90°

N-(2,6-Dimethylphenyl)-2-(2-thienyl)acetamide

C₁₄H₁₅NOS

Ferreira de Lima, Marcelle de Souza, Marcus V. N.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3203

a=4.7489(2)Å b=11.7309(5)Å c=11.8117(4)Å

α=100.981(2)° β=95.427(2)° γ=101.104(2)°

(E)-1-(2,4-Dinitrophenyl)-2-pentylidenehydrazine

C₁₁H₁₄N₄O₄

Neunfeldt, Patrícia D.Duval, Auri R.Cunico, Wilson Wardell, Solange M. S. V.Tiekink, Edward R. T.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 2 o483-o484

a=31.162(3)Å b=4.4930(4)Å c=18.7329(14)Å

α=90° β=106.159(4)° γ=90°

5-{[(E)-2-(4-Iodophenyl)hydrazinylidene]methyl}thiophene-2-carbaldehyde

C₁₂H₉IN₂OS

Wardell, Solange M. S. V.de Lima, Geraldo M.Tiekink, Edward R. T.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 2 o271-o272

a=6.9291(9)Å b=11.7602(10)Å c=30.958(4)Å

α=90° β=90° γ=90°

(4-Benzyl-2-oxo-1,3-oxazolidin-5-yl)methyl methanesulfonate

C₁₂H₁₅NO₅S

Cunico, Wilson Gomes, Claudia R. B.Tiekink, Edward R. T.Vellasco Junior, Walcimar T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 2 o267-o268

a=8.7332(5)Å b=5.8757(3)Å c=12.9650(7)Å

α=90° β=103.317(3)° γ=90°

2-Bromopyridine-3-carboxylic acid

C₆H₄BrNO₂

Howie, R. Alan Gonçalves, Raoni S.de Souza, Marcus V. N.Tiekink, Edward R. T.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 2 o486

a=3.9286(3)Å b=12.9737(9)Å c=12.8570(8)Å

α=90° β=96.695(4)° γ=90°

Benzyl N-[(S)-2-hydroxy-1-({[(E)-2-hydroxy- 4-methoxybenzylidene]hydrazinyl}carbonyl)ethyl]carbamate

C₁₉H₂₁N₃O₆

de Souza, Marcus V. N.Pinheiro, Alessandra C.Tiekink, Edward R. T.Wardell, Solange M. S. V.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 12 o3253-o3254

a=5.1634(2)Å b=32.3173(11)Å c=5.7030(2)Å

α=90° β=103.918(2)° γ=90°

tert-Butyl N-{(1S)-1-[(2,4-dihydroxybenzylidene)hydrazinecarbonyl]- 2-hydroxyethyl}carbamate ethanol monosolvate

C₁₅H₂₁N₃O_6,C₂H₆O

Pinheiro, Alessandra C.de Souza, Marcus V. N.Tiekink, Edward R. T.Wardell, Solange M. S. V.Wardell, James L.

Acta Crystallographica Section E (2011) 67, 3 o581-o582

a=17.4054(4)Å b=8.7266(2)Å c=15.0105(4)Å

α=90° β=122.219(2)° γ=90°

(2E)-N'-Benzoyl-3-(4-nitrophenyl)prop-2-enohydrazide

C₁₆H₁₃N₃O₄

Carvalho, Samir A.da Silva, Edson F.de Souza, Marcus V. N.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 1 o150-o151

a=6.8263(2)Å b=9.6483(3)Å c=10.8571(3)Å

α=95.535(2)° β=102.701(2)° γ=91.728(2)°

N-(4-Bromophenyl)-2-(2-thienyl)acetamide

C₁₂H₁₀BrNOS

Nogueira, Thais C. M.de Souza, Marcus V. N.Wardell, James L.Wardell, Solange M. S. V.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 1 o177

a=4.7517(2)Å b=10.7283(3)Å c=11.7964(3)Å

α=76.419(2)° β=88.437(2)° γ=84.479(2)°

(E)-1-(4-Nitrophenyl)-2-(4-{[(E)-2-(4- nitrophenyl)hydrazinylidene]methyl}benzylidene)hydrazine dihydrate

C₂₀H₁₆N₆O_4,2(H₂O)

Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 1 o191-o192

a=7.7549(4)Å b=9.3245(7)Å c=15.3374(11)Å

α=100.749(3)° β=90.533(4)° γ=103.131(5)°

7-Chloro-4-[(E)-2-(4-methoxybenzylidene)hydrazin-1-yl]quinoline monohydrate

C₁₇H₁₄ClN₃O_,H₂O

de Lima Ferreira, Marcelle de Souza, Marcus V. N.Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 3 o696-o697

a=7.0086(6)Å b=9.2384(8)Å c=13.3701(12)Å

α=100.026(4)° β=103.903(5)° γ=107.000(5)°

Bis(phenylsulfinyl)methane

C₁₃H₁₂O₂S₂

Wardell, Solange M. S. V.de Lima, Geraldo M.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 3 o653-o654

a=8.4368(4)Å b=17.1966(7)Å c=17.1387(6)Å

α=90° β=95.251(3)° γ=90°

fac-(2-Amidoethyl-κ^2^C^1^,O)aquatrichloridotin(IV)—–\ 1,4,7,10,13,16-hexaoxacyclooctadecane (2/1)

2(C₃H₈Cl₃NO₂Sn)_,C₁₂H₂₄O₆

Wardell, Solange M. S. V.Harrison, William T. A.Tiekink, Edward R. T.de Lima, Geraldo M.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 3 m312-m313

a=10.1260(2)Å b=10.0893(3)Å c=15.8229(4)Å

α=90° β=105.814(2)° γ=90°

fac-Aqua(2-carboxyethyl-κ^2^C,O)trichloridotin(IV)—– 1,4,7,10,13-pentaoxacyclopentadecane—–water (1/1/2)

C₁₀H₂₀O_5,C₃H₇Cl₃O₃Sn_,2(H₂O)

Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 5 m496-m497

a=7.2193(2)Å b=29.6516(13)Å c=10.3871(5)Å

α=90° β=91.857(2)° γ=90°

(2E)-N'-[(E)-4-Chlorobenzylidene]- 3-phenylprop-2-enohydrazide monohydrate

C₁₆H₁₃ClN₂O_,H₂O

Carvalho, Samir A.da Silva, Edson F.Fraga, Carlos A. M.Wardell, Solange M. S. V.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 9 o2410-o2411

a=34.078(3)Å b=5.9824(6)Å c=7.2912(6)Å

α=90° β=95.674(3)° γ=90°

2-(4H-1,3-Benzoxazin-2-yl)phenol

C₁₄H₁₁NO₂

Fernandes, Christiane Horn Jr, Adolfo Howie, R. Alan Schripsma, Jan Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2009) 65, 12 o3104-o3105

a=14.1148(8)Å b=5.1725(2)Å c=15.8813(8)Å

α=90.00° β=115.032(2)° γ=90.00°

5-(3-Nitrobenzyl)-1,3,4-thiadiazol-2-amine

C₉H₈N₄O₂S

Carvalho, Samir A.de Feitosa, Larisse O.da Silva, Edson F.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2009) 65, 12 o3200-o3201

a=5.0878(2)Å b=5.6213(3)Å c=17.8035(9)Å

α=80.980(3)° β=85.677(3)° γ=79.855(3)°

Dichloridobis(1,10-phenanthroline-5,6-dione-κ^2^N,N)mercury(II)

C₂₄H₁₂Cl₂HgN₄O₄

Figueiras, Carlos A. L.Bomfim, João A. S.Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.

Acta Crystallographica Section E (2009) 65, 12 m1645

a=8.2261(2)Å b=42.6761(11)Å c=12.6108(3)Å

α=90° β=90° γ=90°

Bis(2-ethoxycarbonylethyl-κ^2^C^1^,O)(2-thioxo-1,3-dithiole- 4,5-dithiolato-κ^2^S^4^,S^5^)tin(IV)

C₁₃H₁₈O₄S₅Sn

de Lima, Geraldo M.Wardell, Solange M. S. V.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2009) 65, 12 m1635-m1636

a=12.1224(2)Å b=13.3825(2)Å c=11.9228(2)Å

α=90° β=90° γ=90°

N'-[(E)-2,6-Dichlorobenzylidene]pyrazine-2-carbohydrazide

C₁₂H₈Cl₂N₄O

Howie, R. Alan de Souza, Marcus V. N.Wardell, Solange M. S. V.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 1 o178-o179

a=6.9325(3)Å b=24.5997(13)Å c=7.6136(4)Å

α=90° β=111.709(3)° γ=90°

7-Chloro-4-[(E)-N'-(4-fluorobenzylidene)hydrazinyl]quinoline monohydrate

C₁₆H₁₁ClFN_3,H₂O

de Souza, Marcus V. N.Howie, R. Alan Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 1 o152-o153

a=3.7795(2)Å b=15.4188(11)Å c=24.8576(16)Å

α=90° β=90.286(4)° γ=90°

1-[2-(Carboxymethoxy)phenyl]-N-(4-chlorophenyl)methanimine oxide

C₁₅H₁₂ClNO₄

Skakle, Janet M. S.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 1 o45-o46

a=7.6631(2)Å b=19.3034(5)Å c=9.6305(3)Å

α=90° β=107.0830(10)° γ=90°

(E)-1-(3-Nitrophenyl)-2-({5-[(1E)-2-(3-nitrophenyl)hydrazin-1- ylidenemethyl]-2-thienyl}methylidene)hydrazine

C₁₈H₁₄N₆O₄S

de Lima, Geraldo M.Harrison, William T. A.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 2 o457-o458

a=11.1790(5)Å b=20.6993(9)Å c=8.0334(2)Å

α=90° β=100.513(2)° γ=90°

tert-Butyl N-[(S)-1-hydrazinecarbonyl-2-hydroxyethyl]carbamate

C₈H₁₇N₃O₄

Pinheiro, Alessandra C.de Souza, Marcus V. N.Wardell, Solange M. S. V.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 4 o994

a=6.9274(5)Å b=5.0074(4)Å c=16.2388(15)Å

α=90° β=94.483(5)° γ=90°

Benzyl N-((S)-2-hydroxy-1-{N'-[(E)- 2-methoxybenzylidene]hydrazinecarbonyl}ethyl)carbamate

C₁₉H₂₁N₃O₅

Pinheiro, Alessandra C.de Souza, Marcus V. N.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2010) 66, 4 o1004-o1005

a=6.002(6)Å b=14.053(14)Å c=21.09(2)Å

α=90° β=90° γ=90°

N-(4-Chlorophenyl)ethanimidamide

C₈H₉ClN₂

Boechat, Nubia Kover, Warner B.Ferreira, Sabrina B.Wardell, Solange M. S. V.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 4 o958

a=9.6460(9)Å b=9.0192(4)Å c=19.3281(5)Å

α=90° β=90° γ=90°

Bis(μ-diphenylarsine-κ^2^As:As)bis[tetracarbonyltungsten(0)]

C₃₂H₂₀As₂O₈W₂

Tiekink, Edward R. T.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 4 m364

a=9.7052(4)Å b=20.1288(7)Å c=16.6450(7)Å

α=90° β=102.835(2)° γ=90°

Methyl 1-{4-[(S)-2-(methoxycarbonyl)pyrrolidin-1-yl]- 3,6-dioxocyclohexa-1,4-dien-1-yl}pyrrolidine-2-carboxylate

C₁₈H₂₂N₂O₆

Garden, Simon J.Skakle, Janet M. S.Tiekink, Edward R. T.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 8 o2071

a=11.4728(5)Å b=7.1556(4)Å c=11.7882(7)Å

α=90° β=111.230(3)° γ=90°

Benzyl N-{(1S)-2-hydroxy-1-[N'-(2- nitrobenzylidene)hydrazinylcarbonyl]ethyl}carbamate

C₁₈H₁₈N₄O₆

de Souza, Marcus V. N.Pinheiro, Alessandra C.Tiekink, Edward R. T.Wardell, Solange M. S. V.Wardell, James L.

Acta Crystallographica Section E (2010) 66, 8 o2023-o2024

a=4.6675(7)Å b=5.7001(7)Å c=16.645(3)Å

α=90.457(9)° β=92.087(7)° γ=97.319(9)°

N-(4-Bromophenyl)pyrazine-2-carboxamide

C₁₁H₈BrN₃O

de Lima Ferreira, Marcelle de Souza, Marcus V. N.Wardell, Solange M. S. V.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 11 o2722-o2723

a=5.8396(4)Å b=7.3317(7)Å c=13.3362(12)Å

α=101.670(4)° β=96.728(5)° γ=110.524(5)°

N-(2-Chloroethyl)pyrazine-2-carboxamide

C₇H₈ClN₃O

da Silva Lima, Camilo H.de Souza, Marcus V. N.Wardell, Solange M. S. V.Wardell, James L.Tiekink, Edward R. T.

Acta Crystallographica Section E (2010) 66, 11 o2886-o2887

a=4.4639(2)Å b=10.6865(6)Å c=17.3583(9)Å

α=90.00° β=93.028(3)° γ=90.00°

2-{[2,8-Bis(trifluoromethyl)quinolin-4-yl](hydroxy)methyl}piperidin-1-ium 3-amino-5-nitrobenzoate sesquihydrate

C₁₇H₁₇F₆N₂O_,C₇H₅N₂O_4,1.5(H₂O)

de Souza, Marcus V. N.Wardell, James L.Wardell, Solange M. S. V.Ng, Seik Weng Tiekink, Edward R. T.

Acta Crystallographica Section E (2011) 67, 11 o3019-o3020

a=9.1705(5)Å b=12.5446(9)Å c=12.7788(8)Å

α=66.278(4)° β=77.261(4)° γ=71.537(4)°

(2-Carbamoylethyl-κ^2^C^1^,O)triiodidotin(IV)

C₃H₆I₃NOSn

de Lima, Geraldo M.Tiekink, Edward R. T.Wardell, James L.Wardell, Solange M. S. V.

Acta Crystallographica Section E (2011) 67, 11 m1536-m1537

a=7.85300(10)Å b=10.62640(10)Å c=14.1250(2)Å

α=98.8010(10)° β=105.5230(10)° γ=102.3830(10)°

tert-Butyl N-((1S)-2-hydroxy-1-{N'-[(1E)- 4-methoxybenzylidene]hydrazinecarbonyl}ethyl)carbamate

C₁₆H₂₃N₃O₅

Pinheiro, Alessandra C.de Souza, Marcus V. N.Tiekink, Edward R. T.Wardell, Solange M. S. V.Wardell, James L.

Acta Crystallographica Section E (2011) 67, 7 o1805-o1806

a=5.3323(4)Å b=5.7200(4)Å c=14.3319(10)Å

α=79.919(4)° β=83.686(4)° γ=76.505(4)°

Benzyl N-(1-{N'-[(E)-2- chlorobenzylidene]hydrazinecarbonyl}-2-hydroxyethyl)carbamate

C₁₈H₁₈ClN₃O₄

de Souza, Marcus V. N.Pinheiro, Alessandra C.Tiekink, Edward R. T.Wardell, Solange M. S. V.Wardell, James L.

Acta Crystallographica Section E (2011) 67, 7 o1868-o1869

a=4.6804(4)Å b=5.6037(7)Å c=16.946(2)Å

α=95.669(6)° β=95.886(7)° γ=94.467(6)°

Benzyl N-(2-hydroxy-1-{N'-[(1E)-2- hydroxybenzylidene]hydrazinecarbonyl}ethyl)carbamate

C₁₈H₁₉N₃O₅

Tiekink, Edward R. T.de Souza, Marcus V. N.Pinheiro, Alessandra C.Wardell, Solange M. S. V.Wardell, James L.

Acta Crystallographica Section E (2011) 67, 7 o1866-o1867

a=5.0338(5)Å b=31.357(3)Å c=5.5882(6)Å

α=90.00° β=97.890(3)° γ=90.00°

2-{1-[2,8-Bis(trifluoromethyl)quinolin-4-yl]-3,5,6,7,8,8a-hexahydro- 1H-1,3-oxazolo[3,4-a]pyridin-3-yl}phenol

C₂₄H₂₀F₆N₂O₂

Gonçalves, Raoni S. B.Kaiser, Carlos R.de Souza, Marcus V. N.Wardell, James L.Wardell, Solange M. S. V.Tiekink, Edward R. T.

Acta Crystallographica Section E (2011) 67, 7 o1656-o1657

a=27.2766(11)Å b=34.1005(9)Å c=9.4431(2)Å

α=90° β=90° γ=90°

N'-[(E)-2-Methoxybenzylidene]pyrazine-2-carbohydrazide

C₁₃H₁₂N₄O₂

de Souza, Marcus V. N.da Lima, Camilo H.Wardell, James L.Wardell, Solange M. S. V.Tiekink, Edward R. T.

Acta Crystallographica Section E (2011) 67, 7 o1714-o1715

a=7.7615(6)Å b=6.4257(4)Å c=12.2480(9)Å

α=90.00° β=93.893(3)° γ=90.00°

2-{(E)-1-[2-(2-Nitrophenyl)hydrazin-1-ylidene]ethyl}benzene-1,3-diol monohydrate

C₁₄H₁₃N₃O_4,H₂O

Howie, R. Alan Wardell, James L.Wardell, Solange M. S. V.Tiekink, Edward R. T.

Acta Crystallographica Section E (2012) 68, 3 o765-o766

a=7.6448(6)Å b=21.405(2)Å c=8.5755(7)Å

α=90.00° β=106.976(5)° γ=90.00°

7-Chloro-4-[(E)-2-(2,5-dimethoxybenzylidene)hydrazin-1-yl]quinoline

C₁₈H₁₆ClN₃O₂

de Souza, Marcus V. N.de Ferreira, Marcelle Wardell, Solange M. S. V.Tiekink, Edward R. T.Wardell, James L.

Acta Crystallographica Section E (2012) 68, 4 o1244-o1245

a=10.5183(2)Å b=12.9132(3)Å c=12.9861(2)Å

α=90.00° β=112.723(2)° γ=90.00°

4-[(E)-2-(2,4-Dichlorobenzylidene)hydrazin-1-yl]quinolin-1-ium chloride monohydrate

C₁₆H₁₂Cl₂N_3,Cl_,H₂O

Wardell, Solange M. S. V.Tiekink, Edward R. T.Wardell, James L.de Ferreira, Marcelle de Souza, Marcus V. N.

Acta Crystallographica Section E (2012) 68, 4 o1232-o1233

a=7.6815(2)Å b=9.7491(3)Å c=10.8418(3)Å

α=87.831(2)° β=87.171(2)° γ=87.146(2)°

3,3-Dimethyl-cis-9a,13a-diphenyl-2,3,9a,11,12,13a-hexahydro-1H-benzo[h][1,4]dioxino[2',3':5,6][1,4]dioxino[2,3-f]chromene

C₃₁H₂₈O₅

Bernardes, Bauer O.Ferreira, Aurelio B. Buarque Wardell, James L.Wardell, Solange M. S. V.Netto-Ferreira, José C.Tiekink, Edward R. T.

Acta Crystallographica Section E (2013) 69, 9 o1487-o1488

a=15.1335(6)Å b=9.6048(2)Å c=16.9739(6)Å

α=90.00° β=97.3840(10)° γ=90.00°

Potassium trifluorido(4-methoxyphenyl)borate

K_,C₇H₇BF₃O

Harrison, William T. A.Wardell, James L.

Acta Crystallographica Section E (2014) 70, 8 68-71

a=7.1347(2)Å b=17.2819(7)Å c=7.3289(3)Å

α=90.00° β=90.00° γ=90.00°

Potassium trifluorido(4-fluorophenyl)borate

K_,C₆H₄BF₄

Harrison, William T. A.Wardell, James L.

Acta Crystallographica Section E (2014) 70, 8 68-71

a=7.1317(5)Å b=7.3757(5)Å c=29.129(2)Å

α=90.00° β=90.00° γ=90.00°